GB-DSC101 High-Temperature Differential Scanning Calorimeter - Hylec Controls

GB-DSC101 High-Temperature Differential Scanning Calorimeter

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Precision Thermal Analysis for High-Temperature Materials

Product Overview

The GB-DSC101 from GBPI is a specialised High-Temperature Differential Scanning Calorimeter designed to meet the rigorous testing demands of high-temperature material characterisation. Operating up to 800∘C800^\circ\mathrm{C}, this instrument seamlessly combines an extensive temperature range with ultra-high sensitivity, intelligent PID temperature control, and rapid cooling capabilities.

Whether you are analysing metals, glass, organic resins, or advanced composites, the GB-DSC101 delivers precise, repeatable thermal data for research, development, and quality control.

Key Features & Advantages

  • Advanced Furnace Structure: Features a new furnace body design utilising indirect conduction. This ensures superior baseline stability, high temperature uniformity, reduced pulse radiation, and a marked performance improvement over traditional heating methods.
  • Ultra-High Sensitivity: Achieves a temperature sensitivity of 0.001∘C0.001^\circ\mathrm{C}, driven by a highly corrosion-resistant and temperature-resistant constant sensor for impeccable measurement accuracy.
  • Intelligent Two-Way Control: Offers seamless operation via both the host device and dedicated software, maximising laboratory efficiency and flexibility.
  • Automated Atmosphere Management: Built-in dual gas switching path operates with rapid switching speeds and minimal stabilisation time. It natively includes a separate input for protective gases.
  • Intuitive Touchscreen Operation: Equipped with a 7-inch, high-clarity color touchscreen interface that displays comprehensive real-time information.
  • Dynamic Temperature Programming: Multi-segment temperature settings allow users to easily configure custom heating, isothermal holding, and cooling cycles tailored to specific material requirements.
  • Powerful Analytical Software: Real-time test spectrum recording, online data analysis, and direct report generation and printing.
  • Customisable Configurations: Instrument parameters can be tailored to meet unique industry testing needs.

Technical Specifications

Parameter Specification
Temperature Range Room Temperature ~ 800∘C800^\circ\mathrm{C}
Temperature Resolution 0.001∘C0.001^\circ\mathrm{C}
Temperature Fluctuation ±0.001∘C\pm 0.001^\circ\mathrm{C}
Temperature Repeatability ±0.01∘C\pm 0.01^\circ\mathrm{C}
Heating Rate 0.10.1 ~ 100∘C/min100^\circ\mathrm{C}/\text{min}
Constant Temperature Time Arbitrarily set
Temperature Control PID control, fully automatic program control (heating/constant)
DSC Range 00 ~ ±800 mW\pm 800\text{ mW}
DSC Resolution 0.001 mW0.001\text{ mW}
Atmosphere Device Built-in float flow meter (mass flow meter optional); dual gas switching
Data Acquisition Frequency 33 points per second (adjustable at multiple points)
Working Power Supply AC220V/50Hz (Customization available)

Application Capabilities & Sample Testing

The GB-DSC101 excels at isolating critical thermal transitions including melting points, enthalpies, and glass transitions (Tg).

Standard Aluminum Melting Point Test

Through standard testing, the GB-DSC101 accurately maps the phase change of solid aluminum to liquid. The detailed spectrum effectively highlights:

  • Starting Point: The temperature at which the sample begins its solid-to-liquid transition (used for factory calibration).
  • Peak Value: The stage of most violent melting.
  • Ending Point: Complete conversion to a liquid state.
  • Result: In standard testing, the melting point is captured at exactly 650.15∘C650.15^\circ\mathrm{C} with an enthalpy value of 397.2713 J/g397.2713\text{ J/g}.

Melting Point & Glass Transition of Barium Silicon Glass/Organic Resin

Complex composites can be mapped precisely across a wide temperature spectrum. The GB-DSC101 tracks multiple distinct thermal events in a single run:

  • Initial Glass Transition: Observed at approximately 247∘C247^\circ\mathrm{C} (corresponding to the Tg of the organic resin).
  • Endothermic Reactions: A significant endothermic peak at 332.06∘C332.06^\circ\mathrm{C} (enthalpy change ≈33.9 J/g\approx 33.9\text{ J/g}) indicating phase transition/decomposition, followed by a secondary peak at 417.62∘C417.62^\circ\mathrm{C}.
  • High-Temperature Glass Transition: Successfully records the glass transition of Barium Silicate glass at ∼644.34∘C\sim 644.34^\circ\mathrm{C}.